| Introduction | p. 1 |
| Theoretical Aspects | p. 5 |
| Nuclear Spins and Energy States | p. 5 |
| A Collection of Spinsùthe Vector Model | p. 10 |
| NMR Parameters | p. 12 |
| Chemical Shift | p. 12 |
| Spin-Multiplicity and Coupling Constant | p. 13 |
| Signal Intensity | p. 16 |
| Nuclear Relaxation | p. 17 |
| NOE | p. 18 |
| Pulsed Fourier Transform NMR | p. 20 |
| Rotational Frame of Reference (RFR) | p. 20 |
| The Single-Pulse Experiment | p. 22 |
| Pulses | p. 25 |
| Non-Selective Pulses | p. 26 |
| Selective Pulses | p. 26 |
| Composite Pulses | p. 27 |
| Shaped Pulses | p. 29 |
| Field Gradient Pulses (PFG) | p. 30 |
| Useful Pulse Sequences | p. 31 |
| Spin-echo | p. 31 |
| Spin-Lock | p. 31 |
| Polarisation Transfer | p. 32 |
| Spectral Editing | p. 33 |
| Two-Dimensional (2D) NMR Spectroscopy | p. 35 |
| The Principle | p. 35 |
| The Appearance of 2D NMR Spectra | p. 38 |
| Description of a Simple 2D NMR Experiment | p. 39 |
| Types of 2D NMR Experiments | p. 41 |
| Solid-State NMR | p. 45 |
| Line-Broadening Factors | p. 45 |
| Removal of Dipolar Coupling and CSA | p. 47 |
| MRI | p. 50 |
| Spatial Encoding and Decoding | p. 50 |
| Basic Imaging Techniques | p. 55 |
| Basic MRI Scans | p. 57 |
| Time Domain (TD) NMR | p. 57 |
| TD NMR Methods | p. 58 |
| Further Reading | p. 64 |
| Liquid-State NMR | p. 64 |
| Solid-State NMR | p. 65 |
| Magnetic Resonance Imaging | p. 65 |
| References | p. 65 |
| Instrumentation | p. 67 |
| The NMR Spectrometer | p. 67 |
| The Magnet | p. 67 |
| The Probe | p. 70 |
| The Console | p. 73 |
| Sensitivity of the NMR Experiment | p. 75 |
| Technological Advances to Improve NMR Sensitivity | p. 76 |
| High-Throughput NMR | p. 77 |
| Technological Advances | p. 77 |
| Hyphenated NMR (LC-NMR) | p. 78 |
| TD NMR | p. 81 |
| References | p. 82 |
| Sample Preparation | p. 84 |
| Sampling | p. 84 |
| Foodstuff Pre-treatment | p. 85 |
| Conservation | p. 85 |
| Removal of Extraneous Matter | p. 85 |
| Reduction | p. 86 |
| Drying | p. 86 |
| Sample Extraction | p. 86 |
| Extraction | p. 86 |
| LLE | p. 87 |
| Microwave Assisted Extraction (MAE) | p. 88 |
| SPE | p. 89 |
| LLE versus SPE | p. 91 |
| NMR Samples Preparation | p. 91 |
| Liquid-State NMR | p. 92 |
| NMR Solvent Selection | p. 93 |
| Solid-State NMR | p. 93 |
| MRI | p. 94 |
| References | p. 94 |
| Experimental Conditions and Processing | p. 96 |
| Qualitative Liquid NMR | p. 96 |
| Setting Up the High-Resolution 1D NMR Experiment | p. 97 |
| Setting Up the 2D NMR Experiment | p. 106 |
| Data Processing | p. 108 |
| Quantitative NMR | p. 116 |
| 1D NMR | p. 116 |
| 2D NMR | p. 122 |
| References | p. 124 |
| Chemometrics in Food Analysis | p. 126 |
| Why Chemometrics? | p. 126 |
| Before the Application of Chemometrics | p. 127 |
| Sample Selection | p. 127 |
| Sample Preparation | p. 128 |
| Data Pre-Processing | p. 128 |
| Targeted or Metabolic Profiling | p. 130 |
| The Chemometric Approach or Metabolic Fingerprinting | p. 131 |
| Chemometric Techniques | p. 132 |
| Unsupervised Pattern Recognition Methods | p. 133 |
| Supervised Pattern Recognition Methods | p. 135 |
| Validation of Chemometric Methods | p. 144 |
| Which Statistical Method to Choose for Food Analysis? | p. 146 |
| References | p. 147 |
| Fats and Oils | p. 149 |
| Vegetable Fats and Oils | p. 149 |
| Triacylglycerols | p. 149 |
| Minor Compounds | p. 156 |
| Quality Assessment | p. 164 |
| Authentication | p. 171 |
| Geographical Origin and Cultivar | p. 173 |
| Animal Oils and Fats | p. 175 |
| Milk Fat | p. 175 |
| Margarines and Hydrogenated Fats | p. 181 |
| Fish Oils 184 References | p. 195 |
| Wine and Beverages | p. 202 |
| Alcoholic Beverages | p. 202 |
| Wine | p. 202 |
| Vinegar | p. 210 |
| Beer | p. 213 |
| Spirits | p. 217 |
| Non-Alcoholic Beverages | p. 219 |
| Coffee | p. 219 |
| Cocoa | p. 223 |
| Tea | p. 225 |
| Juices 228 References | p. 233 |
| Fruits and Vegetables | p. 241 |
| Fruits | p. 241 |
| Composition and Metabolite Profiling | p. 241 |
| Growth and Ripening | p. 244 |
| Quality Evaluation | p. 249 |
| Processing | p. 254 |
| Vegetables | p. 260 |
| Compositional Analysis and Metabolite Profiling | p. 260 |
| Quality Evaluation | p. 264 |
| Processing | p. 267 |
| References | p. 271 |
| Milk and Dairy Products | p. 280 |
| Milk | p. 280 |
| Composition and Metabolite Profiling | p. 280 |
| Quality and Processing | p. 283 |
| Cheese | p. 285 |
| Composition and Metabolite Profiling | p. 285 |
| Quality and Processing | p. 287 |
| Yogurt | p. 290 |
| Ice Cream | p. 290 |
| References | p. 291 |
| Meat | p. 295 |
| Composition and Metabolite Profiling | p. 295 |
| Quality | p. 298 |
| Post Mortem Metabolism | p. 298 |
| Water Holding Capacity | p. 301 |
| Processing | p. 302 |
| Freezing | p. 302 |
| Cooking | p. 303 |
| Curing | p. 304 |
| References | p. 306 |
| Subject Index | p. 310 |
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