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Multivariate Calibration - Harald Martens

Multivariate Calibration

Paperback Published: 7th August 1992
ISBN: 9780471930471
Number Of Pages: 438

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Multivariate Calibration Harald Martens, Chemist, Norwegian Food Research Institute, Aas, Norway and Norwegian Computing Center, Oslo, Norway Tormod Naes, Statistician, Norwegian Food Research Institute, Aas, Norway The aim of this inter-disciplinary book is to present an up-to-date view of multivariate calibration of analytical instruments, for use in research, development and routine laboratory and process operation. The book is intended to show practitioners in chemistry and technology how to extract the quantitative and understandable information embedded in non-selective, overwhelming and apparently useless measurements by multivariate data analysis. Multivariate calibration is the process of learning how to combine data from several channels, in order to overcome selectivity problems, gain new insight and allow automatic outlier detection. Multivariate calibration is the basis for the present success of high-speed Near-Infrared (NIR) diffuse spectroscopy of intact samples. But the technique is very general: it has shown similar advantages in, for instance, UV, Vis, and IR spectrophotometry, (transmittance, reflectance and fluorescence), for x-ray diffraction, NMR, MS, thermal analysis, chromatography (GC, HPLC) and for electrophoresis and image analysis (tomography, microscopy), as well as other techniques. The book is written at two levels: the main level is structured as a tutorial on the practical use of multivariate calibration techniques. It is intended for university courses and self-study for chemists and technologists, giving one complete and versatile approach, based mainly on data compression methodology in self-modelling PLS regression, with considerations of experimental design, data pre-processing and model validation. A second, more methodological, level is intended for statisticians and specialists in chemometrics. It compares several alternative calibration methods, validation approaches and ways to optimize the models. The book also outlines some cognitive changes needed in analytical chemistry, and suggests ways to overcome some communication problems between statistics and chemistry and technology.

Computational and Statistical Problems and Tools.

Methods for Calibration.

Assessment, Validation and Choice of Calibration Method.

Outlier Detection.

Data Selection and Experimental Design.

Pretreatment and Linearization.

Multivariate Calibration Illustrated: Quantifying Litmus in Dirty Samples.

References.

Symbols and Abbreviations.

Index and Cross Reference List.

ISBN: 9780471930471
ISBN-10: 0471930474
Audience: Professional
Format: Paperback
Language: English
Number Of Pages: 438
Published: 7th August 1992
Country of Publication: GB
Dimensions (cm): 24.1 x 16.05  x 2.59
Weight (kg): 0.63
Edition Number: 1

Earn 966 Qantas Points
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