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Materials Syntheses

A Practical Guide

By: Ulrich Schubert (Editor), Nicola Hüsing (Editor), Richard Laine (Editor)

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Hardcover | 2 July 2008

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240 Pages

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24.13 x 16.51 x 1.91

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Materials syntheses are generally more complex than syntheses of inorganic or organic compounds, and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. A number of detailed protocols has been collected, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis.

Each contribution provides detailed and unambiguous description of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful.

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Non-Fiction Engineering & Technology Mechanical Engineering & Materials Materials Science Science Chemistry Inorganic Chemistry Organic Chemistry Physical Chemistry Technology in General Nanotechnology

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Published: 13th October 2010

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Preface	p. 1
List of Contributors	p. 3
Controlling Size and Morphology of Zeolite L	p. 9
Large Zeolite L Crystals	p. 11
Medium-sized Disc-shaped Zeolite L Crystals	p. 13
Nano-sized Zeolite L Crystals	p. 15
Medium-sized Cylindrical-shaped Zeolite L Crystals	p. 16
Zeolite A and ZK-4	p. 21
Zeolite A Crystals	p. 25
ZK-4 Crystals	p. 26
Nano-sized Zeolite A Crystals (Fig. 4)	p. 27
Mesostructured Silica Thin Films	p. 29
Preparation of the Coating Sol	p. 32
Film Deposition	p. 33
Post Treatment	p. 33
Organically Modified Monolithic Silica Aerogels	p. 39
Preparation of 3-Methacryloxypropyl-substituted Silica Aerogel	p. 41
Preparation of 2-Aminoethyl-3-aminopropyl-substituted Silica Aerogel	p. 44
Porous Silica Gel by Acid Leaching of Metakaolin	p. 47
Preparation of Metakaolins	p. 49
Preparation of the Acid-activated Solids	p. 49
Zirconia-Pillared Clays	p. 53
Preparation of Zr-pillared Clays Using Zirconyl Chloride as Precursor	p. 55
Preparation of Zr-pillared Clays Using Zirconium Acetate as Precursor	p. 57
Montmorillonites with Mixed Aluminum-Lanthanide Oxide Pillars	p. 59
Preparation of the Pillaring Agent	p. 60
Pillaring Process	p. 61
Birnessite-type Manganese Oxide by Redox Precipitation	p. 65
Redox Precipitation	p. 67
Hydrothermal Treatment	p. 68
Templated Carbon from Pyrolysis of Pyrene in Pillared Clay Matrices	p. 71
Preparation of Pillared Clay	p. 73
Loading of the Pillared Clay with Organic Compounds	p. 74
Pyrolysis, and Removal of the Inorganic Matrix	p. 75
Fiberous Carbon from Sepiolite Clay and Propylene	p. 77
Preparation of Propylene-loaded Sepiolite	p. 79
Pyrolysis and Dissolution of the Propylene-loaded Sepiolite	p. 81
Aerosol Spray Synthesis of Porous Molybdenum Sulfide Powder	p. 83
Preparation of Low-porosity MoS[subscript 2]	p. 86
Preparation of Porous MoS[subscript 2]	p. 86
Sonochemically Prepared Molybdenum Sulfide	p. 89
Preparation in Glove Box	p. 91
Reaction in Fume Hood	p. 92
Product Isolation	p. 92
Doped Manganites	p. 95
Preparation of La[subscript 0.5]Ba[subscript 0.5]MnO[subscript 3]	p. 97
Preparation of La[subscript 0.5]Sr[subscript 0.5]MnO[subscript 3]	p. 100
Lithium Manganese Oxide Prepared by Flux Methods	p. 103
Growth of LiMn[subscript 2]O[subscript 4] Spinel Single Crystals in a LiCl-Mn(NO[subscript 3])[subscript 2] Flux	p. 105
Growth of LiMn[subscript 2]O[subscript 4] Spinel Single Crystals in a LiCl-MnCl[subscript 2] Flux	p. 107
Nanoscale Magnesium Oxide	p. 111
Nanostructured Pt-doped Tin Oxide Films	p. 117
Preparation of Tetra(tert-butoxy)tin	p. 119
Preparation of the Sol for Coating	p. 119
Film Deposition and Annealing	p. 121
Organically Functionalized Silica Nanoparticles	p. 127
Synthesis of SiO[subscript 2] Nanoparticles	p. 129
Preparation of 2-[4-(Chloromethyl)phenyl]ethyltriethoxysilane	p. 130
Functionalization of the Silica Particles	p. 130
Copper Nanoparticles in Silica	p. 135
Sol-Gel Processing of Alkoxysilyl-substituted Metal Complexes	p. 138
Oxidation	p. 139
Reduction	p. 140
Copper Nanocrystals	p. 143
Assembly of TOPO-Capped Silver Nanoparticles to Multilayered Films	p. 149
Preparation of Silver Hydrosols	p. 151
Transfer of the Silver Nanoparticle Sol into Organic Solvents	p. 151
Multilayered Film Synthesis	p. 152
Colloidal Dispersion of Gold Nanoparticles	p. 155
Preparation of HAuCl[subscript 4 middle dot]3H[subscript 2]O	p. 157
Preparation of Gold Nanoparticles Colloidal Suspension	p. 158
One-dimensional Nanorods and Nanowires	p. 163
Preparation of Gold Seeds	p. 164
Preparation of Growth Solution	p. 164
Preparation of Gold Nanorods and Wires	p. 165
Monolithic Tin-doped Silica Glass	p. 169
Sol Preparation	p. 171
Sol-Gel Transition and Drying	p. 171
Thermal Treatment and Glass Formation	p. 172
Sintering Process A	p. 172
Sintering Process B	p. 173
Octaphenyloctasilsesquioxane and Polyphenylsilsesquioxane for Nanocomposites	p. 179
Synthesis of Phenyltriethoxysilane (PTES)	p. 182
Synthesis of OPS and its Polymeric Analog PPS from PTES	p. 182
Polysilsesquicarbodiimide Xerogels	p. 193
Polyaniline - A Conducting Polymer	p. 199
Preparation of Polyaniline Hydrochloride	p. 201
Preparation of Polyaniline Base	p. 204
Allyl- and Hydroxytelechelic Poly(isobutylenes)	p. 209
Syntheses of Allyl-telechelic PIB (1)	p. 213
Syntheses of Hydroxyl-telechelic PIBs (2)	p. 215
Symmetrically and Unsymmetrically Substituted Phthalocyanines	p. 217
Procedure A	p. 221
Procedure B	p. 223
Index	p. 227
Table of Contents provided by Ingram. All Rights Reserved.

Materials Syntheses

A Practical Guide

At a Glance

Hardcover

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How to return your order

Defective items

You Can Find This Book In

Other Editions and Formats

Paperback

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