Flow Injection Analysis : Instrumentation and Applications

Instrumentation and Applications

By: Marek Trojanowicz

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Hardcover | 1 December 1999

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Hardcover
496 Pages

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22.23 x 16.51 x 2.54

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The concept of flow injection analysis (FIA) was introduced in the mid-seventies. It was preceded by the success of segmented flow analysis, mainly in clinical and environmental analysis. This advance, as well as the development of continuous monitors for process control and environmental monitors, ensured the success of the FIA methodology. As an exceptionally effective means of mechanization for various procedures of wet chemical analysis, the FIA methodology, in use with a whole arsenal of detection methods of modern analytical chemistry, proved to be of great interest to many.The fast and intensive development of the FIA methodology was due to several factors essential for routine analytical determinations, such as very limited sample consumption, the short analysis time based on a transient signal measurement in a flow-through detector and an on-line carrying out difficult operations of separation, preconcentration or physicochemical conversion of analytes into detectable species.Twenty-year studies by numerous research groups all over the world have provided significant progress in the theoretical description of dispersion phenomena in FIA and various operations of physicochemical treatment of the analyte. This volume is devoted to the presentation of the current status of development of the instrumentation for FIA and the many fields of its practical applications, based on an extensive bibliography of original research publications.

Industry Reviews

"... the book contains much beneficial information. It will certainly prove most helpful as a handbook for practising chemists ..." Trends in Analytical Chemistry, 2001

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Non-Fiction Engineering & Technology Technology in General Engineering in General Biochemical Engineering Science Chemistry Analytical Chemistry Booktopia Publisher Services World Scientific Publishing

Introduction	p. xi
Molecular Spectroscopy Detection	p. 1
Visible Absorption Spectrophotometry	p. 1
Detectors	p. 2
Measuring Procedures	p. 6
Kinetic Methods of Detection	p. 19
Determination of Gaseous Analytes	p. 22
Multicomponent Determinations	p. 24
FIA or Liquid Chromatography?	p. 30
Detection in the Ultraviolet Region	p. 31
Infrared Detection	p. 35
Turbidimetric Detection	p. 36
Molecular Luminescence Detection Methods	p. 40
Fluorimetric Detection	p. 40
Chemiluminescence Detection	p. 46
Other Molecular Spectroscopic Detection Methods	p. 50
References	p. 53
Atomic Spectroscopy Detection Methods	p. 68
Atomic Absorption Spectroscopy	p. 68
Flow Injection Systems with Flame Atomisation	p. 69
Electrothermal Atomisation	p. 85
Measurements Involving Conversion of the Analyte into the Gaseous Phase	p. 89
Atomic Emission Spectroscopy	p. 93
Flame Photometry	p. 93
Emission Spectroscopy Based on Plasma Sources	p. 94
Atomic Fluorescence Spectroscopy	p. 99
References	p. 100
Electrochemical Detection Methods	p. 107
Potentiometric Detection	p. 107
Properties of Potentiometric Detectors in FIA	p. 107
Construction of Detectors	p. 112
Measuring Techniques	p. 117
Amperometric Detection	p. 126
Principle of Detection	p. 127
Flow-Through Cells and Electrode Materials	p. 129
Measuring Procedures	p. 134
Scanning and Stripping Methods	p. 143
Voltammetric Detection	p. 143
Voltammetric Stripping	p. 145
Potentiometric Stripping	p. 150
Conductometric Detection	p. 151
Flow Injection Coulometry	p. 152
References	p. 154
Enzymatic Methods of Detection and Immunoassays	p. 162
Enzymatic Assays	p. 163
Systems with Soluble Enzymes	p. 163
Systems with Immobilised Enzyme Reactors	p. 165
Biosensors as Detectors in FIA	p. 177
Multicomponent Enzymatic Assays	p. 181
Determination of Enzyme Activity	p. 184
Determinations Based on Inhibition of Enzyme Activity	p. 185
Flow Injection Immunoassays	p. 188
Immunoprecipitation	p. 188
Fluoroimmunoassays	p. 188
Enzyme Immunoassays	p. 191
References	p. 194
Other Detection Methods Used in Fia	p. 202
Photoacoustic Spectroscopic Detection	p. 202
Flow Injection Inductively Coupled Plasma Mass Spectrometry	p. 203
FIA in the Gaseous Phase	p. 205
References	p. 207
On-Line Sample Processing in Fia Systems	p. 209
Irradiation Procedures	p. 209
Dialysis	p. 212
Gas Diffusion	p. 216
Solvent Extraction	p. 223
Solid-Phase Extraction	p. 236
Flow-Through Reactors	p. 247
Precipitation	p. 252
Less Common Operations	p. 257
References	p. 258
Speciation Analysis Using Flow Injection Methodology	p. 271
Speciation of the Oxidation State of Elements	p. 273
Determination of the Degree of Complexation	p. 288
Speciation of Organometallic Compounds	p. 290
References	p. 294
Applications of Flow Injection Methods in Routine Analysis	p. 298
Environmental Applications	p. 298
Inland Tap Waters	p. 299
Non-specific Water Quality Parameters	p. 299
Inorganic Macrocomponents	p. 301
Inorganic Microcomponents	p. 305
Organic Compounds	p. 318
Sea Water	p. 320
Wastes	p. 325
Sediments	p. 335
Air and Aerosols	p. 337
Food Analysis	p. 338
Fruit Juices and Soft Drinks	p. 338
Milk and Dairy products	p. 344
Wine	p. 347
Other Food Products	p. 351
Biological Materials	p. 354
Plants	p. 354
Animal Tissues	p. 359
Mineral Materials	p. 361
Soil	p. 361
Ores, Minerals and Ceramic Materials	p. 365
Fertilisers	p. 370
Alloys	p. 370
Clinical Analysis	p. 372
Serum and Plasma	p. 372
Whole Blood	p. 386
Urine	p. 389
Other Specimens	p. 392
Pharmaceutical Applications	p. 394
Biotechnology	p. 402
Process Analysis	p. 405
Industrial Applications	p. 406
Monitoring of Wastes and Waste Treatment	p. 410
On-Line Monitoring in Biotechnology	p. 411
References	p. 418
Sequential and Batch Injection Techniques	p. 437
Principle of Measurement and Basic Instrumentation of SIA	p. 438
Measurement Techniques and On-Line Sample Pretreatment in SIA	p. 441
Detection Methods in SIA Systems	p. 448
Batch Injection Analysis	p. 451
References	p. 459
Commercially Available Instrumentation for Fia	p. 463
Fia	p. 465
Alitea USA	p. 465
Alpkem	p. 466
Burkard	p. 467
Eppendorf	p. 467
Hitachi	p. 468
Ismatec	p. 471
Lachat	p. 471
Perkin-Elmer	p. 472
Sanuki	p. 473
Tecator	p. 473
Zhaofa	p. 474
SIA	p. 474
References	p. 475
Current Trends in Developments of Flow Analysis	p. 476
Miniaturisation	p. 477
Multicomponent Detection	p. 478
Hyphenation to High-Performance Separation Systems	p. 479
References	p. 480
Table of Contents provided by Syndetics. All Rights Reserved.

Flow Injection Analysis : Instrumentation and Applications

Instrumentation and Applications

At a Glance

Hardcover

Industry Reviews

Shipping

How to return your order

Defective items

You Can Find This Book In

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