Microscale Diagnostic Techniques

By: Kenny Breuer (Editor)

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Hardcover | 12 November 2004

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Hardcover
272 Pages

Dimensions(cm)
23.5 x 15.88 x 1.27

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Microscale Diagnostic Techniques highlights the most innovative and powerful developments in microscale diagnostics. It provides a resource for scientists and researchers interested in learning about the techniques themselves, including their capabilities and limitations. The fields of Micro- and Nanotechnology have emerged over the past decade as a major focus of modern scientific and engineering research and technology. Driven by advances in microfabrication, the investigation, manipulation and engineering of systems characterized by micrometer and, more recently, nanometer scales have become commonplace throughout all technical disciplines. With these developments, an entirely new collection of experimental techniques has been developed to explore and characterize such systems.

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Microrheology	p. 1
Introduction	p. 1
Active Microrheology Methods	p. 2
Magnetic Manipulation Techniques	p. 3
Optical Tweezers Measurements	p. 8
Atomic Force Microscopy Techniques	p. 14
Passive Microrheology Methods	p. 18
Practical Applications of One-Particle Microrheology	p. 28
Two-Particle Microrheology	p. 30
Summary	p. 33
Appendix: Descriptions of Experimental Apparati	p. 34
Dynamic Light Scattering	p. 35
Diffusing Wave Spectroscopy	p. 38
Video Microscopy	p. 39
Obtaining	p. 42
References	p. 44
Micron-Resolution Particle Image Velocimetry	p. 51
Introduction	p. 51
Theory of µPIV	p. 53
In-Plane Spatial Resolution Limits	p. 53
Out-of-Plane Spatial Resolution	p. 55
Particle Visibility	p. 57
Particle/Fluid Dynamics	p. 60
Brownian Motion	p. 62
Saffman Effect	p. 65
Typical Micro-PIV Hardware Implementation	p. 66
Algorithms and Processing for µPIV	p. 67
Processing Methods Most Suitable for µPIV	p. 68
Overlapping of LID-PIV Recordings	p. 68
Correlation Averaging Method	p. 70
Processing Methods Suitable for Both Micro/Macro PIV	p. 73
Central Difference Interrogation	p. 74
Image Correction Technique	p. 75
Application Examples of µPIV	p. 76
Flow in a Microchannel	p. 76
Flow in a Micronozzle	p. 82
Flow Around Blood Cell	p. 85
Flow in Microfluidic Biochip	p. 87
Extensions of the µPIV Technique	p. 89
Microfluidic Nanoscope	p. 90
Micro-Particle Image Thermometry	p. 96
Infrared µPIV	p. 107
Conclusions	p. 109
References	p. 110
Electrokinetic Flow Diagnostics	p. 113
Theory	p. 114
Electroosmosis	p. 115
Electrophoresis	p. 119
Similarity Between Electric Field and Velocity Field for Fluid.120
Diagnostics	p. 121
Capillary Electrophoresis: Electrokinetic System Background	p. 121
Simple Dye Visualization	p. 130
Photobleached Fluorescence Visualization	p. 133
Caged-Fluorescence Visualization	p. 137
Particle Imaging Techniques	p. 141
Concluding Remarks	p. 149
References	p. 150
Micro- and Nano-Scale Diagnostic Techniques for Thermometry and Thermal Imaging of Microelectronic and Data Storage Devices.	p. 155
Introduction	p. 155
State-Of-Art Technologies and Relevant Thermal Phenomenon in Semiconductor Devices	p. 157
State-Of-Art Technologies and Relevant Thermal Phenomena in Data Storage Technologies	p. 160
Thermometry	p. 162
Electrical Thermometry	p. 162
Far-Field Optical Thermometry	p. 166
Near-Field Thermometry Techniques	p. 175
Summary and Recommendations	p. 188
References	p. 189
Nanoscale Mechanical Characterization of Carbon Nanotubes	p. 197
Introduction	p. 197
Instruments for Nanoscale Characterization	p. 198
Atomic Force Microscope (AFM)	p. 198
Scanning Tunneling Microscope (STM)	p. 199
Transmission Electron Microscope (TEM)	p. 200
Scanning Electron Microscope (SEM)	p. 200
New Tools for SEM201
New Tools for TEM	p. 206
New Tools for AFM	p. 209
Techniques for Nanoscale Mechanical Characterization of CNT	p. 211
Tensile Testing Method	p. 211
AFM Lateral Deflection and Indentation Method	p. 213
Mechanical Resonance Method	p. 217
Other Methods	p. 219
Mechanical Engineering Applications of Individual CNTs for Actuation and Electromechanics	p. 221
Conclusion and Future Directions	p. 222
References	p. 223
Applications of the Piezoelectric Quartz Crystal Microbalance for Microdevice Development	p. 227
Introduction	p. 227
Properties of Piezoelectric Quartz	p. 228
Theoretical Models	p. 229
Theory for Thin Films and Purely Elastic Media	p. 230
Example Calculation: Quartz Crystal Preparation	p. 231
Transmission-Line Model	p. 232
Theory for Purely Viscous Media	p. 233
Theory for Viscoelastic Media	p. 234
Theory Including Gases at Low Pressures	p. 235
Theory Combining Mass (Thin Film) and Semi-continuous Fluid Loading	p. 236
Theory Incorporating Slip at the Interface	p. 236
Theory for Combined Viscous Film, Slip, and Semicontinuous Vapor	p. 237
Equipment and Experimental Methods	p. 238
Equipment	p. 238
Experimental Considerations	p. 238
Experimental Observations of Slip at Interfaces	p. 240
Slip of Adsorbed Monolayers of Gases	p. 241
Liquid Phase Slip	p. 242
Measurement of Viscoelastic Properties of Films	p. 244
Moduli Measurements	p. 244
Solvent Dynamics	p. 244
Tribology and Tribochemistry of Surfaces	p. 245
Friction and Wear in MEMS	p. 245
Combined QCM/Surface Probe Instruments	p. 246
QCM Uses in Physiological Processes	p. 250
Detection and Characterization of Cell Adhesion	p. 250
Protein and Lipid Adsorption	p. 251
References	p. 254
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Microscale Diagnostic Techniques

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