Electrocrystallization

Fundamentals of Nucleation and Growth

By: Alexander Milchev

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Hardcover | 30 June 2002

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284 Pages

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23.5 x 15.88 x 1.91

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This is an up-to-date introduction to the fundamentals of the initial stages of electrocrystallization, which are dominated by nucleation and growth of the first clusters of the new phase. It offers a readable exposition of the topic, in simple terms, providing a detailed theoretical description of the phenomena involved. The most relevant aspects of the experimental studies of electrochemical nucleation and growth are considered, as well, including some important methods for acquiring and analyzing experimental results. Having specific properties quite different from those of bulk materials, these small, nano-clusters have always attracted considerable attention, and many sophisticated methods have been developed for cluster studies. In spite of this, information on small clusters can still be obtained by simple experiments, and the book shows that electrocrystallization is unique in this respect. In this special case the phase change may be controlled experimentally by controlling the voltage and current, two simple and easily measurable electrical quantities. Certainly, this is what makes electrochemical systems an attractive object of study both from a scientific and from a practical point of view. The book is suitable not only for specialists in Electrocrystallization but also for graduate and PhD students, as well as for scientists from diverse but related fields like pure and applied electrochemistry, electrocatalysis, corrosion, electrochemical adsorption and materials science.

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Preface	p. ix
Thermodynamics of Electrochemical Nucleation	p. 1
General concepts	p. 1
Nucleation work	p. 11
Theory of mean sepration works	p. 46
Atomistic considerations	p. 68
Kinetics of Electrochemical Nucleation	p. 83
General formulation	p. 83
Classical theory of stationary nucleation	p. 89
Atomistic theory of stationary nucleation	p. 106
Non-stationary nucleation	p. 128
Stochastic Approach to Nucleation	p. 165
Temporal distribution of clusters	p. 165
Spatial distribution of clusters	p. 177
Electrochemical Crystal Growth	p. 189
Growth of an individual crystal face	p. 189
Growth of a hemispherical liquid drop	p. 203
Mass Electrocrystallization	p. 219
General concepts	p. 219
Progressive and instantaneous nucleation without overlap	p. 220
Progressive and instantaneous nucleation with overlap	p. 228
Author Index	p. 255
Subject Index	p. 263
Table of Contents provided by Syndetics. All Rights Reserved.

Electrocrystallization

Fundamentals of Nucleation and Growth

At a Glance

Hardcover

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