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Reaction Detection in Liquid Chromatography : Chromatographic Science Series - Ira S. Krull

Reaction Detection in Liquid Chromatography

Chromatographic Science Series

By: Ira S. Krull (Editor)

Hardcover Published: 1st August 1986
ISBN: 9780824775797
Number Of Pages: 377

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The first book to focus entirely on reactions for analyte detection and characterization, Reaction Detection in Liquid Chromatography depicts off- and on-line, pre- and post-column approaches that have been successfully used for many classes of compounds, both organic and inorganic, in high performance liquid chromatography. The book gives special attention to methods and instrumentation associated with post-column reaction detection, discussing theory, background, principles, and equations ... and also highlights major areas of reaction chemistry, such as immobilized (or solution) enzymatic reactions, homogenous solution chemistry, photochemical derivation, pairedion reagents, solid phase and solid supported reagents, and reactions for inorganic species. In addition, Reaction Detection in Liquid Chromatography details the efficiencies of the various reactions surveyed ... forecasts how the utility of each reaction is likely to be enhanced by new research ... and gives data that will allow the reader to reproduce reaction-detection approaches for new analytes and samples. Reaction Detection in Liquid Chromatography is essential reading for analytical, bioanalytical, quality control, and research and development chemists. It also comprises a fine reference for analysts involved in development and applications of liquid chromatography for specific qualitative and quantitative analyte identification; and in-house, professional seminars. Book jacket.

Prefacep. iii
Acknowledgmentsp. v
Contributorsp. ix
Fundamentals of Reaction Detection Systemsp. 1
Introductionp. 1
Instrumentationp. 3
Dispersion in Open Tubular Reactor Systemsp. 8
Dispersion in Packed-Bed Reactorsp. 38
Comparison of the Different Reactor Typesp. 46
List of Symbolsp. 53
Referencesp. 54
Solution Chemistry for Post-Column Reactionsp. 63
Introductionp. 63
Instrumentationp. 64
Post-Column Reagentsp. 69
Post-Column Applicationsp. 77
Recent Developmentsp. 107
Future Developmentsp. 117
Referencesp. 119
Post-Column Reaction Detection of Inorganic Speciesp. 129
Introductionp. 129
Designp. 132
Chemistryp. 145
Applicationsp. 157
Conclusionsp. 189
Referencesp. 190
Enzyme Reaction Detectors in HPLCp. 195
Introductionp. 195
Analytical Considerations in the Use of Enzymesp. 196
Tandem HPLC-Immobilized Enzyme Systemsp. 207
Applicationsp. 215
Summaryp. 220
Referencesp. 222
Solid-Phase Reaction Detectors for HPLCp. 227
Introductionp. 227
Construction of Solid-Phase Reactorsp. 234
Polymeric Solid-Phase Reactorsp. 235
Nonpolymeric Solid-Phase Reactorsp. 247
Commercial Solid-Phase Reaction Systemsp. 251
Referencesp. 254
Ion Pairing as a Means of Detection in Liquid Chromatographyp. 259
Introductionp. 259
Backgroundp. 261
Prechromatographic Counterion Additionp. 262
Postchromatographic Counterion Additionp. 269
Conclusionsp. 297
Referencesp. 298
Post-Column Photochemical Derivatizations for Improved Detection and Identification in HPLCp. 303
Introductionp. 303
Post-Column Photochemical Derivatizations for Improved HPLC-UV and HPLC-FL Detectionp. 307
Post-Column Photochemical Derivatizations for Improved HPLC-EC Detection (HPLC-hv-EC)p. 321
The Photoconductivity Detector in HPLC (HPLC-PCD)p. 334
The Photoionization Detector in HPLCp. 336
The Photoelectrochemical Detector in HPLCp. 340
Conclusions and Recommendations for Future Research and Developmentp. 343
Referencesp. 347
Author Indexp. 353
Subject Indexp. 359
Table of Contents provided by Ingram. All Rights Reserved.

ISBN: 9780824775797
ISBN-10: 0824775791
Series: Chromatographic Science Series
Audience: Professional
Format: Hardcover
Language: English
Number Of Pages: 377
Published: 1st August 1986
Country of Publication: US
Dimensions (cm): 23.42 x 15.8  x 2.29
Weight (kg): 0.67
Edition Number: 1

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