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Organozinc Reagents : A Practical Approach - Paul Knochel

Organozinc Reagents

A Practical Approach

By: Paul Knochel (Editor), Philip Jones (Editor)

Hardcover Published: 23rd November 1998
ISBN: 9780198501213
Number Of Pages: 354

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A comprehensive and conveniently organized lab manual containing step-by-step experimental procedures and the major aspects of organozinc compounds. The world-renowned contributors also cover the diverse roles these reagents play in contemporary organic synthesis. The initial chapters give full details, including experimental procedures, for the preparation of a wide range of organozinc reagents involving classical methods, and procedures involving active zinc, modern electrolysis, and ultrasound. The subsequent chapters give comprehensive coverage of the applications of organozinc reagents in organic synthesis, including cyclopropanation reactions, transition-metal catalyzed reactions, and the use of organozinc reagents in asymmetric synthesis. The Reformatsky and Barbier reactions are dealt with in detail, giving an up-to-date overview of these classical reactions.
Organozinc Reagents: A Practical Approach concludes with two very useful appendices: A compilation of organozin reagents and a list of suppliers. Written in a clear and convenient format, this new volume in the
Oxford Practical Approach Series in Chemistry will prove a valuable methods reference for postgraduate chemists, researchers, and professionals in industrial chemistry and chemists involved in organic synthesis.

"Overall, this book is a superb summary of current trends in organozinc chemistry. The discussion is kept to a minimum, yet it provides helpful comments from many authors. Together with the clear diagrams, it provides excellent background material for those new to the area. The detailed procedures are the key feature of this book and should result in organozinc reagents having an even greater role in synthetic chemistry in the future. I recommend this book to all those either currently using or considering organozinc reagents."Chemistry in Britain, ' It provides much valuable practical guidance ... The appendix contains a valuable treasure in the form of a compilation of original literature references on about 333 organozinc reagents ... this book is a must for the preparative organic chemist who wishes to use organozinc reagents in synthetic work and wants a source of reliable and reproducible laboratory protocols' Angew Chem. Int Ed

1. Organozinc Chemistry: An Overview and General Experimental Guidelines 2. Activated Zinc in Organic Synthesis 3. Preparation Methods of Organozinc Halides 4. Fluorinated Organozinc Reagents 5. Preparation Methods of Diorganozincs 6. Preparation and Reaction of Triorganozincates 7. Preparation and Reactions of 1,n-bimetallic reagents 8. Electrochemical Generation and Reactions of Zinc Reagents 9. Uncatalyzed Reactions of Zinc Organometallics 10. Copper, Titanium, Manganese, Cobalt and Iron Catalyzed Reactions of Zinc Organometallics 11. Palladium and Nickel Catalyzed Reactions of Zinc and Copper Organometallics 12. Asymmetric Additions using Diorganozincs 13. Cyclopropanations Mediated by Zinc Organometallics 14. The Reformatsky Reaction 15. Zinc Mediated Barbier Reactions Appendix 1: Compilation of Organozinc Reagents Appendix 2: List of Suppliers

ISBN: 9780198501213
ISBN-10: 0198501218
Series: Practical Approach in Chemistry
Audience: Professional
Format: Hardcover
Language: English
Number Of Pages: 354
Published: 23rd November 1998
Country of Publication: GB
Dimensions (cm): 24.28 x 16.41  x 2.69
Weight (kg): 0.65

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