Nanohybridization of Organic-Inorganic Materials

By: Atsushi Muramatsu (Editor), Tokuji Miyashita (Editor)

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Hardcover | 23 November 2009

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306 Pages

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Synthesis and application of nanoparticles have been often reported by researchers in material science, chemistry and physics. While nanoparticles themselves are well known to exhibit fascinating characteristics. interest in their improvement and promotion is now turning to the hybridization of organic and/or inorganic nano-materials. Although nano-level hybridization is an outstandingly novel and original technique, it encounters many difficulties to achieving the desired industrial application. To thoroughly review the research in this field, this book focuses on the synthesis, characterization and process of nano-hybrid materials, including nanoparticles and ultra-thin films.

It elucidates the fundamental aspects of nano-hybrid materials in the synthesis procedure, characterization, and processes with selected examples, from both the basic science and the engineering appications points of view. In fact, this is the first comprehensive compilation of new advances that covers the current status and topics of new synthetic information of nano-hybrid materials composed of organic and/or inorganic materials at the nano-meter level, in one volume. As such, the book provides a unique source of information and guidance for specialists and non-specialists alike.

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Non-Fiction Engineering & Technology Mechanical Engineering & Materials Materials Science Science Chemistry Physical Chemistry Technology in General Engineering in General Nanotechnology Industrial Chemistry & Manufacturing Technologies Industrial Chemistry

Surface-Coating Technology

Nanohybridization of Nanoparticles
Nanohybridized Synthesis of Metal Nanoparticles and Their Organization	p. 3
Introduction	p. 3
Design of Nanoparticle-Based Building Blocks	p. 4
Stabilized by Thiol Ligand	p. 5
Stabilized by Amine Ligands	p. 7
Stabilized by Bipyridyl Ligands	p. 8
Stabilized by Phosphine Ligands	p. 8
Controlling Numbers of Functional Group on Nanoparticle Building Blocks	p. 9
Well-Defined Nanoparticle Hybrids with Linear Polymers	p. 10
Polymer-Grafted Metal Nanoparticles	p. 10
¿-Conjugated Polymer Metal Nanoparticle Hybrids	p. 12
Organization of Metal Nanoparticles	p. 13
Overview of Metal Nanoparticle Organizations	p. 13
Organization of Metal Nanoparticles by Dendritic Molecules	p. 15
Self-Organized Nanocomposites	p. 19
Organic-Metal ID Nanostructures	p. 25
Flocculation of Metal Nanoparticles by Stimuli	p. 27
Photoresponsive Aggregation	p. 27
Metal Nanoparticles Modified with an Ionic Liquid Moiety	p. 28
Conclusion and Outlook	p. 32
References	p. 33
Organic-Inorganic Hybrid Liquid Crystals: Innovation Toward ôSuprahybrid Materialö	p. 41
Materials Innovation Toward ôSuprahybrid Materialö by the Utilization of Organic-Inorganic Hybridization	p. 41
Organic Liquid Crystals and Lyotropic Liquid-Crystalline Inorganic Fine Particles	p. 42
Development of Organic-Inorganic Hybrid Liquid Crystals	p. 44
Hybridization of Calamitic Liquid-Crystalline Amines with Monodispersed TiO2 Nanoparticles [4]	p. 44
Hybridization of Calamitic Liquid-Crystalline Phosphates with Monodispersed ¿-Fe2O3 Fine Particles [5]	p. 48
Summary and Prospect	p. 51
References	p. 52
Polymer-Assisted Composites of Trimetallic Nanoparticles with a Three-Layered Core-Shell Structure for Catalyses	p. 55
Introduction	p. 55
Fabrication of a Core/Shell Structure	p. 56
Fabrication of Pd/Ag/Rh Trimetallic Nanoparticles	p. 59
Catalytic Properties of Pd/Ag/Rh Trimetallic Nanoparticles	p. 64
Au/Pt/Rh Trimetallic Nanoparticles	p. 68
Pt/Pd/Rh Trimetallic Nanoparticles	p. 74
Concluding Remarks	p. 76
References	p. 78
Fabrication of Organic Nanocrystals and Novel Nanohybrid Materials	p. 81
Introduction	p. 81
PDA Nanocrystals	p. 83
Fabrication Technique: Reprecipitation Method	p. 83
Optical Properties of PDA Nanocrystals	p. 87
Hybridized PDA Nanocrystals	p. 88
Silver-Deposited PDA Nanocrystals Fabricated Using Surfactants as Binder	p. 88
Silver-Deposited PDA Nanocrystals Produced by Visible-Light-Driven Photocatalytic Reduction	p. 94
Summary and Future Scopes	p. 98
References	p. 99
Nanohybridized Thin Films
Polymer Nanoassemblies and Their Nanohybridization with Metallic Nanoparticles	p. 103
Introduction	p. 103
Hybrid Nanoassemblies via Polymer Nanosheets	p. 106
Spectroscopic Properties of Hybrid-Assemblies	p. 1ll
Hybrid Polymer Nanosheet Fabricated from Core-Shell Nanoparticles	p. 114
Synthesis of Magnetic Nanoparticle Covered with Poly(N-Alkylmethacrylamide)s	p. 115
Monolayer Behavior of p(alkylMA)s-Coated Iron Oxide Nanoparticles at the Air-Water Interface	p. 116
Surface Morphology of Nanoparticle Monolayer at Different Deposition Pressures	p. 119
Multilayer Formation	p. 120
Conclusion	p. 121
References	p. 122
Single Molecular Film for Recognizing Biological Molecular Interaction: DNA-Protein Interaction and Enzyme Reaction	p. 125
Introduction	p. 125
Surface Forces Measurement	p. 125
Interaction Between Nucleic Acid Bases	p. 126
Surface Immobilization of Protein Modified with His-Tag	p. 127
pH Dependence of DSIDA Interactions	p. 129
Interactions Between DSIDA Monolayers in the Presence of Cu2+	p. 130
AFM Imaging of Immobilized His-Tag Sigma A Protein	p. 130
Specific Interactions Between Enzyme-Substrate Complexes: Heptaprenyl Diphosphate Synthase	p. 130
Interaction Between Subunit I and Subunit II upon Approach	p. 131
Interaction Between Subunit I and Subunit II upon Separation	p. 132
Selectivity in Substrate-Enzyme Complexation	p. 134
Sequence-Dependent Interaction Between a Transcription Factor and DNA	p. 136
Conclusion	p. 136
References	p. 136
Nanohybridized Fine Porous Materials
Organic-Inorganic Hybrid Mesoporous Silica	p. 141
Introduction	p. 141
Postsynthetic Grafting Methods	p. 142
Direct Synthesis from Monosilylated Organic Precursors	p. 143
Direct Synthesis from Polysilylated Organic Precursors	p. 146
Synthesis of PMOs from 100% Polysilylated Organic Precursors	p. 147
Synthesis of PMOs by Cocondensation	p. 152
PMOs with Crystal-Like Pore Walls	p. 157
Synthesis of Various PMOs with Crystal-Like Pore Walls	p. 158
Synthesis of PMO with Crystal-Like Pore Walls Obtained from Allyl Precursors	p. 161
Functionalization of PMO with Crystal-Like Pore Walls	p. 163
Summary	p. 164
References	p. 165
Organic-Inorganic Hybrid Zeolites Containing Organic Frameworks	p. 171
Introduction	p. 171
Synthesis and Physical Properties of ZOL	p. 172
Crystallization Scheme	p. 180
Proof of Organic Framework	p. 183
Applications and Prospects	p. 188
References	p. 189
Characterization and Process of Nanohybridized Materials
Characterization of Metal Proteins	p. 193
Introduction	p. 193
Proteins and Metals	p. 193
Metals in Biology	p. 195
Iron (Fe)	p. 196
Copper (Cu)	p. 197
Zinc (Zn)	p. 197
Calcium (Ca)	p. 198
Special Metal Cofactors	p. 199
Iron-Sulfur Cofactor	p. 199
Hemes	p. 201
Functions of Metalloproteins	p. 202
O2 Transport	p. 202
Electron Transfer	p. 202
Structural Roles for Metal Ions	p. 203
Function of Metalloenzymes	p. 203
Physical Methods in Characterizing Metalloproteins	p. 204
X-Ray Crystallography	p. 204
Optical Absorption Spectroscopy	p. 207
X-Ray Absorption Spectroscopy	p. 209
Vibrational Spectroscopy	p. 210
Electron Paramagnetic Resonance spectroscopy	p. 211
Nuclear Magnetic Resonance Spectroscopy	p. 212
Mössbauer Spectroscopy	p. 213
General References	p. 215
References	p. 216
Electron Microscopy Characterization of Hybrid Metallic Nanomaterials	p. 219
Introduction	p. 219
Principles of Electron Microscopy	p. 219
Transmission Electron Microscopy	p. 219
High-Angle Annular Dark-Field STEM	p. 223
Analytical Electron Microscopy	p. 224
Electron Holography	p. 227
Specimen Preparation	p. 230
Ultramicrotomy	p. 230
Ion Milling	p. 231
Focused Ion Beam	p. 232
Applications	p. 233
Carbon-Metal System (Carbon-Encapsulated Metal Nanoparticles)	p. 233
Oxide-Oxide System (YBa2Cu3Oy High-Tc Superconductor)	p. 236
Metal-Based Compound System (Nd-Fe-B Nanocomposite Magnet)	p. 238
Metal-Oxide System (Co-CoO Recording Tape)	p. 239
Polymer-Metal System (Silver-Epoxy Paste)	p. 242
References	p. 245
Supercritical Hydrothermal Synthesis of Organic-Inorganic Hybrid Nanoparticles	p. 247
Introduction	p. 247
Supercritical Hydrothermal Technique	p. 249
Apparatus	p. 251
Basic Principles of Supercritical Hydrothermal Synthesis	p. 253
Supercritical Hydrothermal Synthesis of Metal Oxides	p. 258
Supercritical Hydrothermal Synthesis of Hybrid Organic-Inorganic Nanoparticles	p. 262
Organic-Inorganic Hybrid Nanoparticles	p. 262
Supercritical Hydrothermal Organic-Inorganic Hybrid Nanoparticles	p. 263
Mechanism of Formation of Organic-Inorganic Hybrid Nanoparticles	p. 265
Experimental Study of the Supercritical Hydrothermal Synthesis of Organic-Inorganic Hybrid Nanoparticles with Size and Shape Control	p. 268
Dispersibility of Organic-Inorganic Hybrid Nanoparticles	p. 271
Evaluation Techniques for Organic Ligand Molecules in Organic-Inorganic Hybrid Nanoparticles	p. 273
Self-Assembly of Hybrid Organic-Inorganic Nanoparticle	p. 274
Conclusion	p. 276
References	p. 277
Index	p. 281
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Nanohybridization of Organic-Inorganic Materials

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