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Multidimensional Solid-State NMR and Polymers : Anthropology, Culture and Society (Hardcover) - Klaus Schmidt-Rohr

Multidimensional Solid-State NMR and Polymers

Anthropology, Culture and Society (Hardcover)

Hardcover Published: 29th November 1994
ISBN: 9780126266306
Number Of Pages: 496

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NMR spectroscopy is the most valuable and versatile analytical tool in chemistry. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. Multidimensional techniques enable researchers to obtain detailed information about the structure, dynamics, orientation, and phase separation of solids, which provides the basis of a better understanding of materials properties on the molecular level.Dramatic progress-much of it pioneered by the authors-has been achieved in this area, especially in synthetic polymers. Solid-state NMR now favorably competes with well-established techniques, such as light, x-ray, or neutron scattering, electron microscopy, and dielectric and mechanical relaxation.
The application of multidimensional solid-state NMR inevitably involves use of concepts from different fields of science. This book also provides the first comprehensive treatment of both the new experimental techniques and the theoretical concepts needed in more complex data analysis. The text addresses spectroscopists and polymer scientists by treating the subject on different levels; descriptive, technical, and mathematical approaches are used when appropriate. It presents an overview of new developments with numerous experimental examples and illustrations, which will appeal to readers interested in both the information content as well as the potential of solid-state NMR. The book also contains many previously unpublished details that will be appreciated by those who want to perform the experiments. The techniques described are applicable not only to the study of synthetic polymers but to numerous problems in solid-state physics, chemistry, materials science, and biophysics.
Key Features
* Presents original theories and new perspectives on scattering techniques
* Provides a systematic treatment of the whole subject
* Gives readers access to previously unpublished material
* Includes extensive illustrations

Introduction
Principles of NMR of Organic Solids
High-Resolution NMR Techniques for Solids
Fourier Theory for 1D and 2D NMR
Short Review of Structure and Dynamics of Solid Polymers
Multidimensional Separation and Correlation
Polymer Dynamics: Multidimensional Exchange Experiments
Multidimensional Exchange NMR Above the Glass Transition
Multidimensional Spectra, Correlation Functions, and Stochastic Processes
Time-Domain Signals for Multidimensional Spectra
Multidimensional Exchange Spectra: Simulations, Models, Angle Distributions
Determination of Order in Polymers by Multidimensional NMR
Domain Sizes and Internuclear Distances from Spin Diffusion and Dipolar Couplings
Appendices
Chapter References
Index
Table of Contents provided by Publisher. All Rights Reserved.

ISBN: 9780126266306
ISBN-10: 0126266301
Series: Anthropology, Culture and Society (Hardcover)
Audience: General
Format: Hardcover
Language: English
Number Of Pages: 496
Published: 29th November 1994
Publisher: ACADEMIC PR INC
Country of Publication: GB
Dimensions (cm): 24.74 x 17.12  x 3.05
Weight (kg): 0.85

Earn 335 Qantas Points
on this Book