Mechanical Properties and Deformation Behavior of Materials Having Ultra-Fine Microstructures : Proceedings of the NATO Advanced Study Institute, Porto Novo, Portugal, June 28 - July 10, 1992

By: Don M. Parkin (Editor), Michael Nastasi (Editor), Herbert Gleiter (Editor)

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This book focuses on the emerging class of new materials characterized by ultra-fine microstrucures. The NATO ASI which produced this book was the first international scientific meeting devoted to a discussion of the mechanical properties and deformation behavior of materials having grain sizes down to a few nanometers. Topics covered include superplasticity, tribology, and the supermodulus effect. Review chapters cover a variety of other themes including synthesis, characterization, thermodynamic stability, and general physical properties. Much of the work is concerned with the issue of how far conventional techniques and concepts can be extended toward atomic scale probing. Another key issue concerns the structure of nanocrystalline materials, in particular, what is the structure and composition of the internal boundaries. These ultra-fine microstructures have proved to challenge even the finest probes that the materials science community has today.

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Preface
Fundamental Concepts
Nanostructured Materials	p. 3
Electron Theory Applied to Phases with Low Dimensions	p. 37
Thermodynamics of Nanostructured Materials	p. 53
Structure and Physical Properties
Interfaces and Physical Properties of Nanostructured Solids	p. 81
Interfacial Structures and Properties	p. 107
Grain Boundary Design for Advanced Materials on the Basis of Grain Size Dependence of Grain Boundary Character Distribution (GBCD)	p. 129
Diffraction Analysis of Ultra-Fine Structures; Lattice Deformations in Multilayers and Martensites	p. 135
An Electron Microscopy Study of Ferromagnetism in Small Nickel Particles as a Function of Size	p. 157
Mechanical Response
The Search for the Supermodulus Effect	p. 165
Recent Studies of the Supermodulus Effect	p. 193
Tribology of Materials and the Effect of Microstructure	p. 199
Mechanical Relaxation Spectroscopy of Fine Grained A1 and A1-Alloy Films	p. 229
Hall-Petch Behavior in Nanocrystalline Metals	p. 241
Mechanical Properties of Layered Structures and Thin Films on Substrates	p. 255
The Mechanical Properties of Fine Scale Metallic Materials	p. 287
Structure and Mechanical Properties of Submicrometere-grained Materials Produced by Severe Plastic Deformation	p. 303
Microstructure and Mechanical Properties of Ultra Fine Grained Elemental Metals	p. 309
Microstructure and Mechanical Properties of Electrodeposited Nanocomposites	p. 315
Tensile Behavior of Cold-Rolled NiTi Having an Amorphous-Crystalline Composite Microstructure	p. 323
Indentation Test on Thermotropic Polymers	p. 329
Grid Supported Polyimide and Beryllium Based Soft X-ray Windows - Pressurized Membrane Ductility Considerations	p. 337
Superplasticity
Creep and Superplasticity	p. 345
Superplasticity of Nanostructured Ceramics	p. 361
Superplasticity of Nanophase Intermetallics?	p. 381
Superplasticity of Nanograin Ceramic Films Tested by the Stress Relaxation Method	p. 401
Very High Strain Rate Superplasticity in Near-Nano Scale Aluminum Alloys	p. 407
Nanoindentation
Mechanical Deformation Using Indentation Experiments	p. 417
Nanoindentation with a Surface Force Apparatus	p. 429
Measurement of Fracture Toughness in Thin Films and Small Volumes Using Nanoindentation Methods	p. 449
Hardness of Vapour Deposited Ceramic Coatings Determined by Ultra-Low Load Indentation	p. 463
Sputter Deposition and Characterization of MoSi[subscript 2]/SiC Composite Coatings	p. 469
Hardness and Young's Modulus of Cosputtered Ti-B-N and Hf-B-N Films and Correlations to Their Microstructure and Composition	p. 475
Nanoindentation of Thin Coated Systems	p. 481
Indentation of Semiconductor Superlattices	p. 489
Nanohardness and Chemical Composition of Be Surfaces for Gas Bearing	p. 495
Synthesis and Processing
Synthesis and Processing of Nanostructured Materials	p. 509
Sinter-Forging of Chemically Precipitated Nanocrystalline TiO[subscript 2]	p. 539
Nanocrystalline ZrO[subscript 2] by Crystallization of Amorphous Oxide	p. 547
Compaction of Submicron and Nanocrystalline Al[subscript 2]O[subscript 3]-ZrO[subscript 2] Ceramics	p. 559
Sintering of Nanocrystalline Al[subscript 2]O[subscript 3]: A Study by Photoacoustic Infrared Spectroscopy	p. 565
Reduction of Surface Oxide on Ultra-Fine FeNi Particles	p. 571
Characterization
Atomic Force Microscopy of Polymer Surfaces	p. 581
Crystallization of Nanocrystalline Alloys Studied by Electron Transport, Magnetic and Dilatometric Methods	p. 587
Acoustic Spectroscopy of Iron and Aluminum Thin Films and Fe/Al Multilayers, Anelasticity and Microstructure	p. 593
X-ray Reflectivity Studies of Twist Grain Boundaries	p. 599
STM Study of Microindentations on Oriented Metallic Single Crystals	p. 605
List of Participants (with addresses)	p. 611
Subject Index	p. 619
Table of Contents provided by Blackwell. All Rights Reserved.

Mechanical Properties and Deformation Behavior of Materials Having Ultra-Fine Microstructures : Proceedings of the NATO Advanced Study Institute, Porto Novo, Portugal, June 28 - July 10, 1992

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