| Introduction to Principles and Practice of Mass Spectrometry | p. 1 |
| History of Mass Spectrometry | p. 1 |
| Ionisation of Molecules | p. 3 |
| Ion Separation | p. 18 |
| Ion Detection | p. 22 |
| Metastable Ions, Collision Induced Dissociation and Tandem Mass Spectrometry | p. 23 |
| Scanning Modes | p. 29 |
| References | p. 32 |
| Interpretation of Organic Mass Spectrometric Data | p. 33 |
| Introduction | p. 33 |
| Formation of the Electron Ionisation Mass Spectrum | p. 34 |
| Calibration of the Mass Scale and Determination of Molecular Mass | p. 37 |
| Interpretation of High- and Low-resolution Data | p. 39 |
| An Empirical Approach to the Elucidation of Organic Structures | p. 40 |
| Additional Information from the Mass Spectrum | p. 44 |
| Classical Fragmentation Processes Occurring in EIMS | p. 46 |
| Some Useful Examples of Features of the Mass Spectrum by Chemical Class | p. 52 |
| References | p. 54 |
| Food Flavourings and Taints | p. 55 |
| Introduction | p. 55 |
| Flavour Analyses | p. 63 |
| Taints and Off-flavours | p. 76 |
| Flavour Chemistry | p. 77 |
| Aroma Release From Foods | p. 81 |
| Breath and Body Odours | p. 85 |
| Authentication of Natural and Synthetic Food Components | p. 85 |
| Data Processing and Statistical Analysis | p. 86 |
| References | p. 87 |
| Bioactive Non-nutrients in Foods | p. 93 |
| Introduction | p. 93 |
| Alkaloids | p. 94 |
| Coumarins | p. 105 |
| Cyanogenic Compounds | p. 107 |
| Glucosinolates | p. 109 |
| Mutagenic Heterocyclic Amines Generated by Cooking | p. 114 |
| Mycotoxins | p. 117 |
| Phytoalexins | p. 134 |
| Phenolic Compounds | p. 134 |
| Saponins | p. 153 |
| References | p. 157 |
| Amino Acids, Peptides and Proteins | p. 170 |
| Introduction | p. 170 |
| Chemical and Enzymatic Studies | p. 174 |
| Applications of Mass Spectrometry to Amino Acid, Peptide and Protein Analysis in Food, Nutrition and Agricultural Research | p. 175 |
| The Amino Acid Sequencing of Peptides and Proteins | p. 179 |
| References | p. 187 |
| Lipids | p. 192 |
| Introduction | p. 192 |
| Derived Lipids | p. 193 |
| Simple Lipids | p. 196 |
| Compounds Lipids | p. 203 |
| Lipid Oxidation Products | p. 208 |
| References | p. 210 |
| Sugars and Carbohydrates | p. 213 |
| Introduction | p. 213 |
| Analysis of Sugar Residues: GC/MS of Derivatised Sugars | p. 215 |
| Partially Methylated Alditol Acetate (PMAA) Analysis of Linkage and Sugar Type | p. 216 |
| Recent Methods for the Determination of Molecular Size | p. 217 |
| The Separation of Oligosaccharides by LC/MS | p. 220 |
| Sequence Determination of Oligosaccharides | p. 220 |
| References | p. 223 |
| Quantification and Metabolism of Inorganic Nutrients | p. 225 |
| Introduction | p. 225 |
| Sample Collection and Treatment for Inorganic Mass Spectrometry | p. 226 |
| Quantitative Applications of TIMS | p. 227 |
| Quantitative Applications of ICP-MS | p. 228 |
| Metabolic Studies of Inorganic Nutrients | p. 228 |
| Sample Preparation for Inorganic Mass Spectrometry | p. 230 |
| Mass Spectrometric Techniques for Inorganic Nutrient Studies | p. 231 |
| References | p. 242 |
| Analysis and Metabolism of Vitamins in Foods | p. 244 |
| Introduction | p. 244 |
| Water-soluble Vitamins | p. 245 |
| Fat-soluble Vitamins | p. 258 |
| General Conclusions and Recommendations | p. 268 |
| References | p. 268 |
| Stable Isotope Studies of Organic Macronutrient Metabolism | p. 273 |
| Introduction | p. 273 |
| Mass Spectrometric Techniques Used in Macronutrient Metabolism Studies | p. 273 |
| Protein Metabolism | p. 273 |
| Carbohydrate Metabolism | p. 275 |
| Lipid Metabolism | p. 278 |
| Whole Body Energy Expenditure | p. 279 |
| General Conclusions and Recommended Methods | p. 280 |
| References | p. 281 |
| Pyrolysis Mass Spectrometry of Foods | p. 283 |
| Introduction | p. 283 |
| Practical Aspects of Py/MS | p. 284 |
| Mass Spectrometric Techniques for Analytical Pyrolysis | p. 284 |
| Analysis of Data | p. 285 |
| Selected Applications of Py/MS in Food Studies | p. 285 |
| Conclusions | p. 288 |
| References | p. 290 |
| Subject Index | p. 291 |
| Table of Contents provided by Syndetics. All Rights Reserved. |