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Inorganic Syntheses : v. 32 - Marcetta York Darensbourg

Inorganic Syntheses

v. 32

Hardcover Published: 23rd April 1998
ISBN: 9780471249214
Number Of Pages: 368

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The Inorganic Synthesis Series provides all users of inorganic substances with detailed and foolproof procedures for the preparation of important and timely compounds. This new volume includes information on water-solubilizing ligands for organometallics, labile ligand complexes, and the syntheses of cluster compounds and hydrides.

"Although some chapters are technical and present a fair amount of data, most of the chapters appear to
be intended for a non-specialist audience. It is a handsome volume but regrettably over-priced for a non-academic readership." (Limnology and Oceanography Bulletin, 2011)

"Comprising the synthesis and analysis of the results of the Census of Marine Life this most important book brings together the work of around 2000 scientists from 80 nations around the globe." (World News, 15 February 2011)

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"The ambitious project involved thousands of scientists and led to the discovery of novel creatures such as the hairy yeti crab. The volume addresses the biodiversity of oceans past, present and future, including microorganisms and zooplankton." (Nature, September 2010)

Chapter One LIGANDS FOR WATER-SOLUBILIZING ORGANOMETALLIC COMPOUNDS.

1. (Meta-Sulfonatophenyl)Diphenylphosphine, Sodium Salt and Its Complexes with Rhodium(I), Ruthenium(II), Iridium(1).

2. Syntheses of Water-Soluble Phosphines and Their Transition Metal Complexes.

3. Tris[Tris(Sodium m-sulfonatophenyl)phosphino] Palladium(0)-Enneahydrate.

4. Sulfonated Phosphines.

5. (S,S)-2,3-Bis[Di(m-Sodiumsulfonatophenyl)phosphino]butane-(chiraphosTS) and (S,S)-2,4-Bis[di(m-Sodiumsulfonatophenyl)-phosphinolpentane (BDPPTS).

6. 1,3,5-Triaza-7-phosphatricyclo[3.3.1.13,7]decane and Derivatives.

Chapter Two BIOMIMETIC AND SPECIAL PROPERTY LIGANDS.

7. 2.2':6',2"-Terpyridine.

8. Poly(1-pyrazolyl)alkane Ligands.

9 . Tris[N-(3-tert-butyl)pyrazolyl]methane.

10. Tris[2-(1,4-Diisopropylimidazolyl)]phosphine.

11. Tris[(2-pyridyl)methyl]amine (TPA) and (+)-Bis[(2-pyridyl)-methyl]-l-(2-pyridyl)ethylamine (a-MeTPA).

12. C2-Symmetric 1,4-Diisopropyl-7-R-l,4,7-Triazacyclononanes.

13. N-(2-hydroxyethyl)-3,5-Dimethylpyrazole, a Dinuclear Copper Complex, and N-(2-p-Toluenesulfonylethyl)-3,5-dimethy-pyrazole.

14. N-(2-Mercaptoethyl)-3,5-dimethylpyrazole.

15. 1,5-Diazacyclooctane, Pendant Arm Thiolato Derivatives and [N,N'-Bis(2-Mercaptoethyl)-1,5-Diazacyclooctanato]-nickel(II).

16. Polydentate Thiolate and Selenolate Ligands, RN(CH2,CH2,S(Se)-)2, and Their Dimeric and Mononuclear Ni(II) Complexes.

17. Poly[(methylthio)methyl]borates and Representative Metal Derivative.

18. Polyaza Binucleating Ligands: OBISTREN and OBISDIEN.

19. N,N'.bis(2-hydroxybyl.thylenediamine-N,N'-diacetic acid (HBED).

20. N-Tert-Alkyl-Anilides as Bulky Ancillary Ligands.

21. 1,2-Bis(Dichlorophosphino)-1,2-Dimethylhydrazine and Alkoxy/Aryloxy Derivatives.

22. Tris[(tert-butylamino)-dimethylsilyl]methylsilane and Its Precursors.

Chapter Three TRANSITION METAL COMPLEXES AND PRECURSORS.

23. Facile Synthesis of Isomerically Pure.

24. cis-Bis(benzeneacetonitrile)dichloroplatinum(II) and trans-Bis(benzeneacetonitrile)dichloroplatinum(II).

25. Platinum(II) Complexes of Dimethyl Sulfide.

26. (2,2' :6',2"-Terpyridine) Methylplatinurn(II) Chloride and (l,l0-Phenanthroline)methylchloroplatinum(II).

27. (N,N-Chelate)(olefin)platinum(0) Complexes.

28. Dimethylpalladium(II) and Monomethylpalladium(II) Reagents and Complexes.

29. 2,4-Pentanedionatogold(I) Complexes and 2,4-Pentanedionatothallium.

30. Tetrakis(Pyridine)SiIver(2 + )Peroxydisulfate.

31. One-Pot Synthesis of Tetrahydronium Tris(4,4'-Dicarboxylato-2,2'-Bipyridine)ruthenium(II) Dihydrate.

32. Trichloro[2,2' :6,2"-Terpyridine]ruthenium(III) and Phosphine Ligand Derivatives.

33. Monomeric Tetrahydrofuran-Stabilized Molybdenum(III) Halides.

34. Facial Molybdenum(lI1) Triamine Complexes.

35. High-Valent Mono-(5-Pentamethylcyclopentadienyl)vanadium and Molybdenum Complexes.

36. Monoindenyltrichloride Complexes of Titanium(IV), Zirconium(IV), and Hafnium(IV).

37. Labile Copper(I) Chloride Complexes: Preparation and Handling.

Chapter Four MAIN GROUP AND TRANSITION METAL CLUSTER COMPOUNDS.

38. 7,8-Dicarbaundecaborane(13).

39. Borazine, Polyborazylene, B-Vinylborazine and Poly(B-Vinylborazine).

40. Transition Metal Complexes of the Lacunary Heteropolytungstate, [P2W17O61] 10-.

41. Bis(Triphenylphosphorany1idene)A mmonium µ-Carbonyl-1kC:2kC-Decacarbonyl-1k3C,2k3,3k4C-µ-Hydrido-1k:2k-triangubTriruthenate(1?).

42. Dipotassium Undecacarbonyl Trimetallate(2?) Clusters, K2[M3(CO)11] (M = Ru, Os).

43. [PPN]2[Ru3(CO)11] and [PPN]2[OS3(CO)11], µ-Nitrido-Bis(Triphenylphosphorus) (1 +) Undecacarbonyltriruthenate (2 ?) and Undecacarbonyltriosmate(2 ?).

44. Platinum-Ruthenium Carbonyl Cluster Complexes.

45. Tri(µ-carbonyl)nonacarbonyltetrarhodiu.

46. High Nuclearity Hydridodecaruthenium Clusters.

Chapter Five MAIN GROUP AND TRANSITION METAL HYDRLDES.

47. Dichlorodihydro(N,N,N',N,-Tetraethyl-1,2-ethanediamine-N,N')silicon.

48. Tricarbonyl(hydrido)[1,2-bis(diphenylphosphino)ethane]-manganese as Precursor to Labile Site Derivatives.

49. Pentahydridobis(tricyclohexylphosphine)iridium(V) and trihydridotris (triphenylphosphine)iridium(III).

Chapter Six TITANIUM(1II) CHLORIDE.

(A Correction to Inorganic Syntheses, Vol. 24, pp. 181 (1986).

50. An Active Form of Titanium(II1) Chloride.

Contributor Index.

Subject Index.

Formula Index.

Chemical Abstracts Service Registry Number Index.

ISBN: 9780471249214
ISBN-10: 0471249211
Series: Inorganic Syntheses : Book 32
Audience: Professional
Format: Hardcover
Language: English
Number Of Pages: 368
Published: 23rd April 1998
Country of Publication: US
Dimensions (cm): 23.5 x 16.0  x 2.31
Weight (kg): 0.65
Edition Number: 1