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Experimental Organometallic Chemistry : A Practicum in Synthesis and Characterization - Andrea L. Wayda

Experimental Organometallic Chemistry

A Practicum in Synthesis and Characterization

By: Andrea L. Wayda (Editor), Marcetta Y. Darensbourg (Editor)

Hardcover

Published: 1st September 1998
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Offers the latest synthetic methodology and characterization techniques used in organometallic chemistry. Describes specialized techniques for difficult synthesis, as well as handling and sampling techniques used by leading experimentalists worldwide. Provides timely, useful information for any scientist who handles or characterizes organometallic compounds.

Techniques in Organometallic Chemistry Cannula Techniques HPLC Analysis Low-Temperature Chromatography Column IR Radiation as a Heat Source Techniques in the Handling of Highly Reduced Organometallics Preparation and Isolation of Crystalline Samples Recrystallization Apparatus Apparatus for UV Photochemical Reactions Distillation Flask for Use with a Heating Mantle Greaseless Stillheads Vacuum Line Techniques Assay of Ligand-Derived Gases Semiautomatic Gas Titration Device Multipurpose Vacuum Line Designs Greaseless Double Manifolds and Schlenkware Diverse Synthesis and Purification Procedures Facile and Inexpensive Repair of Drybox Gloves Continuous Inert Gas Purge Glovebox Cooling of Reactions Inside a Glovebox Using Metal Atoms and Molecular High-Temperature Species Heated Inlet System Recovering Air-Sensitive Products Versatile Sonochemical Reaction Vessels Pressure Reactors for Reactivity Studies Characterization of Inorganic and Organometallic Complexes Detection of Dihydrogen Complexes Method for Sealing and Opening NMR Tubes Method for Acquiring IR Spectral Data Simple Low-Temperature Solution IR Cell Quantum Yield Determination Spectrophotometric Cell Handling of Reactive Compounds for X-Ray Structure Analysis In Situ Crystal Growth Photoelectron Spectroscopy

ISBN: 9780841214385
ISBN-10: 0841214387
Series: ACS Symposium Series
Audience: Tertiary; University or College
Format: Hardcover
Language: English
Number Of Pages: 312
Published: 1st September 1998
Publisher: American Chemical Society
Country of Publication: US
Dimensions (cm): 23.5 x 15.9  x 2.0
Weight (kg): 0.56