Enantioselective Electrochemical Câ"H Activation Enabled by Sustainable 3d Transition Metal Catalysis : BestMasters - Sven Erik Peters

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Enantioselective Electrochemical Câ"H Activation Enabled by Sustainable 3d Transition Metal Catalysis

By: Sven Erik Peters

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Paperback | 27 March 2025

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108 Pages

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14.8 x 21.0 x 0.9

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Enantioselective metallaelectro-catalyzed Câ"H activation represents an innovative strategy for enabling the transition of organic synthesis to a more resource-economic mode of operation. It circumvents substrate prefunctionalization by directly exploiting otherwise inert Câ"H bonds to construct complex three-dimensional scaffolds from simple molecular building blocks. Furthermore, the mild electrocatalytic conditions evade chemical oxidants, while producing molecular hydrogen as the sole by-product, enabling the connection of organic synthesis to a possible future decentralized green hydrogen economy.
Still, disclosed methodologies predominantly rely on noble metal catalysts. Examples using earth-abundant 3d transition metals remain scarce despite the substantially improved ecological and economic implications and diminished toxicity. This work addresses this shortcoming by investigating the first enantioselective nickelaelectro-catalyzed Câ"H activation and various cobaltaelectro-catalyzed conversions. On this occasion, the synthetic versatility is examined and various mechanistic experiments are presented for fostering future developments.

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