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Chromatography of Polymers : Characterization by SEC and FFF - Theodore Provder

Chromatography of Polymers

Characterization by SEC and FFF

By: Theodore Provder (Editor)

Hardcover

Published: 1st May 1993
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Covers current developments in sedimentation and thermal field flow fractionation for particle size analysis, and characterization of polymer molecular-weight distribution. Presents fundamental studies on critical conditions in liquid chromatography, single-parameter approach to universal SEC calibration, and compositional characterization of polyolefin copolymers as a function of molecular weight and bunching. Provides a strategy for interpreting multidetector size exclusion chromatography (SEC) data. Reviews SEC for cationic, anionic, and nonionic copolymers of vinylpyrrolidone. Presents applications of SEC for the characterization of natural polymer products, cotton, and polysaccharides.

Preface
Field-Flow Fractionation
Calibration of a Photosedimentometer Using Sedimentation Field-Flow Fractionation and Gas Chromatographyp. 2
Particle-Size Analysis Using Flow Field-Flow Fractionationp. 13
Separation and Characterization of Polymeric Latex Beads and Aggregates by Sedimentation Field-Flow Fractionationp. 30
Polymer Separation and Molecular-Weight Distribution by Thermal Field-Flow Fractionationp. 47
Copolymer Retention in Thermal Field-Flow Fractionation: Dependence on Composition and Conformationp. 63
Gel-Content Determination of Polymers Using Thermal Field-Flow Fractionationp. 77
Size-Exclusion Chromatography: Fundamental Considerations
Critical Conditions in the Liquid Chromatography of Polymersp. 90
Single-Parameter Universal Calibration Curvep. 103
Specific Refractive Index Increments Determined by Quantitative Size-Exclusion Chromatographyp. 113
Copolymer Characterization Using Conventional Size-Exclusion Chromatography and Molar-Mass-Sensitive Detectorsp. 122
Size-Exclusion Chromatography and End-Group Analysis of Poly(methyl methacrylate)p. 149
Size-Exclusion Chromatography: Viscometry Detection
A Strategy for Interpreting Multidetector Size-Exclusion Chromatography Data I: Development of a Systematic Approachp. 180
A Strategy for Interpreting Multidetector Size-Exclusion Chromatography Data II: Applications in Plastic Waste Recoveryp. 199
Single-Capillary Viscometer Used for Accurate Determination of Molecular Weights and Mark - Houwink Constantsp. 220
Gel Permeation Chromatography - Viscometry: Various Solvent Systemsp. 231
Absolute M[subscript n] Determined by Gel Permeation Chromatography - Differential Viscometryp. 243
Size-Exclusion Chromatography: High-Temperature, Ionic, and Natural Polymer Applications
Size-Exclusion Chromatographic Assessment of Long-Chain Branch Frequency in Polyethylenesp. 254
Gel Permeation Chromatography - Fourier Transform IR Spectroscopy To Characterize Ethylene-Based Polyolefin Copolymersp. 270
Molecular-Weight Determination of Poly (4-methyl-1-pentene)p. 277
Size-Exclusion Chromatography of Cationic, Nonionic, and Anionic Copolymers of Vinylpyrrolidonep. 292
Size-Exclusion Chromatography To Characterize Cotton Fiberp. 302
Structural Analysis of Aggregated Polysaccharides by High-Performance Size-Exclusion Chromatography - Viscometryp. 314
Author Indexp. 328
Affiliation Indexp. 328
Subject Indexp. 329
Table of Contents provided by Blackwell. All Rights Reserved.

ISBN: 9780841226258
ISBN-10: 0841226253
Series: ACS Symposium Series
Audience: Professional
Format: Hardcover
Language: English
Number Of Pages: 338
Published: 1st May 1993
Publisher: American Chemical Society
Country of Publication: US
Dimensions (cm): 23.4 x 15.8  x 2.1
Weight (kg): 0.59