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Capillary Electrochromatography : RSC Chromatography Monographs - Keith D. Bartle

Capillary Electrochromatography

RSC Chromatography Monographs

By: Keith D. Bartle (Editor), Peter Myers (Editor), Roger M. Smith (Editor), D.B. Gordon (Contribution by), Gwyn A. Lord (Contribution by)

Hardcover Published: 1st March 2001
ISBN: 9780854045303
Number Of Pages: 166

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Capillary electrochromatography (CEC) is a new and exciting hybrid separation technique that seeks to exploit the combined advantages of both capillary electrophoresis (high efficiencies) and HPLC (mobile and stationary phase selectivity). It is a technique with tremendous potential, especially in the pharmaceutical and biomedical fields. This is the first book to be devoted to the topic and presents reviews by the world leaders in the field on the theory and development of the technique and current and potential future applications. "Capillary Electrochromatography" provides an excellent introduction to the field for graduates and professionals in industry and academia with an interest in separation science. part of the RSC Chromatography Monographs series]

Industry Reviews

"... a compact and informative review of the principles and practice of this novel and exciting technique ... the book will be very useful to readers new to the field as it is both up-to-date and fully referenced ..." * Chemistry & Industry, Issue 1, 7 January 2002, p 19 * "... an excellent introduction to anyone about to enter the field ... useful and highly informative ..." * Angewandte Chemie, International Edition, Vol 41, No 3, 1 February 2002 *

An Introduction to Capillary Electrochromatographyp. 1
What Is Capillary Electrochromatography?p. 1
History of CECp. 2
Electroosmosisp. 5
Classification of CECp. 7
Band-broadening in CECp. 9
Effect of Operating Variables in CECp. 12
Application Areas of CECp. 17
Referencesp. 20
The Capillary Electrochromatographp. 23
Introductionp. 23
Modification of Standard CZE Equipmentp. 23
Sample Injection Using Modified CZE Equipmentp. 27
Modification of CZE Equipment with Autosampler Capabilityp. 28
Commercial CEC Instrumentsp. 29
Future Instrument Designs and Requirementsp. 30
Referencesp. 31
Supports and Stationary Phases for Capillary Electrochromatographyp. 33
Introductionp. 33
Particle Size Distributionsp. 34
The Silica Surfacep. 35
Bonding Technologyp. 36
Effect of pH on the Silanolsp. 37
Analyte Focusingp. 38
Anion Exchange Materialsp. 40
Continuous Bed Columnsp. 40
Conclusionsp. 41
Referencesp. 41
Electroosmosis in Complex Media: Bulk Transport in CECp. 42
Introductionp. 42
Electroosmotic Flowp. 43
Electroosmosis in Packed Bedsp. 47
Electroosmosis in Porous Monolithsp. 60
Conclusionp. 62
Referencesp. 62
Capillary Electrochromatography with Open Tubular Columns (OTCEC)p. 64
Introductionp. 64
Chromatographic Effects in CZEp. 65
Theory of Dispersion and Achievable Efficiency in OTLC and OTCECp. 68
Improving the Phase Ratio for OTCECp. 73
Conclusionsp. 83
Referencesp. 84
Capillary Electrochromatography/Mass Spectrometryp. 87
Introductionp. 87
Mass Spectrometryp. 87
Capillary Electrochromatography/Mass Spectrometry Couplingp. 93
Practical Aspectsp. 100
Future Prospectsp. 104
Referencesp. 105
Pharmaceutical Applications of Capillary Electrochromatographyp. 107
Introductionp. 107
Scope and Applicability of CECp. 108
Pharmaceutical Applications of CECp. 111
Issues Associated with CEC in Pharmaceutical Analysisp. 118
The Future of CEC in the Pharmaceutical Industryp. 121
Referencesp. 122
Capillary Electrochromatography in Natural Product Researchp. 125
Introductionp. 125
Experimentalp. 125
Triglyceridesp. 126
Fatty Acids and Their Derivativesp. 135
CEC Analysis of Other 'Hydrophobic' Samplesp. 142
Conclusionp. 144
Referencesp. 144
Subject Indexp. 146
Table of Contents provided by Syndetics. All Rights Reserved.

ISBN: 9780854045303
ISBN-10: 0854045309
Series: RSC Chromatography Monographs
Audience: Professional
Format: Hardcover
Language: English
Number Of Pages: 166
Published: 1st March 2001
Country of Publication: GB
Dimensions (cm): 24.23 x 16.15  x 1.45
Weight (kg): 0.37

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