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Applications of Solid Phase Microextraction : RSC Chromatography Monographs - Dr. Janusz Pawliszyn

Applications of Solid Phase Microextraction

RSC Chromatography Monographs

By: Dr. Janusz Pawliszyn (Editor), Roger M. Smith (Editor), Kiyokatsu Jinno (Contribution by), John R. Dean (Contribution by), Stefan Weber (Contribution by)

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Applications of Solid Phase Microextraction (SPME) describes the applications of this technique as a modern alternative to current sample preparation technology. In industry, practical uses of SPME can be found in environmental, food, pharmaceutical, clinical and forensic applications, all of which are described in this book. New technologies are presented throughout, including new coatings and interfaces for analytical instrumentation, automation and calibration processes.

Glossary
Calibration and Quantitation by SPME
Quantitative Aspects of SPMEp. 3
Quantitation by SPME before Reaching a Partition Equilibriump. 22
Coatings and Interfaces
SPME Coupled to Capillary Electrophoresisp. 41
Selectivity in SPMEp. 49
Properties of Commercial SPME Coatingsp. 57
Sol-Gel Technology for Thermally Stable Coatings in SPMEp. 73
Solid versus Liquid Coatingsp. 92
Physicochemical Applications
Application of SPME to Study Sorption Phenomena on Dissolved Humic Organic Matterp. 111
The Use of SPME to Measure Free Concentrations and Phospholipid/Water and Protein/Water Partition Coefficientsp. 129
Estimation of Hydrophobicity of Organic Compoundsp. 140
Environmental Applications
Air Sampling with SPMEp. 159
The Application of SPME in Water Analysisp. 169
The Application of SPME to Pesticide Residue Analysisp. 188
Inter-laboratory Validation of SPME for the Quantitative Analysis of Aqueous Samplesp. 201
SPME for the Determination of Organochlorine Pesticides in Natural Watersp. 212
Determination of Sulfur-containing Compounds in Wastewaterp. 227
Analysis of Creosote and Oil in Aqueous Contaminations by SPMEp. 238
Direct Analysis of Solids Using SPMEp. 248
Analysis of Solid Samples by Hot Water Extraction-SPMEp. 258
Field Analysis by SPMEp. 269
Organometallic Speciation by Combining Aqueous Phase Derivatization with SPME-GC-FPD-MSp. 284
Metal Speciation by SPME-CGC-ICPMSp. 296
The Application of SPME-LC-MS to the Determination of Contaminants in Complex Environmental Matricesp. 311
SPME-HPLC of Environmental Pollutantsp. 327
Analysis of Industrial Pollutants in Environmental Samplesp. 333
Food, Flavour, Fragrance and Pheromone Applications
Analysis of Food and Plant Volatilesp. 349
Application of SPME to Measure Volatile Metabolites Produced by Staphylococcus carnosus and Staphylococcus xylosusp. 364
Application of SPME Methods for the Determination of Volatile Wine Aroma Compounds in View of the Varietal Characterizationp. 372
Analysis of Vodkas and White Rums by SPME-GC-MSp. 393
Analysis of Food Volatiles Using SPMEp. 407
Analysis of Volatile Contaminants in Foodsp. 423
Determination of Pesticides in Foods by Automated SPME-GC-MSp. 435
SPME in the Study of Chemical Communication in Social Waspsp. 448
Pharmaceutical, Clinical and Forensic Applications
Propyl Chloroformate Derivatisation and SPME-GC for Screening of Amines in Urinep. 461
Isolation of Drugs and Poisons in Biological Fluids by SPMEp. 470
On-fiber Derivatization for Analysis of Steroids by SPME and GC-MSp. 486
SPME-Quadrupole Ion Trap Mass Spectrometry for the Determination of Drugs of Abuse in Biological Matricesp. 497
Analysis of Drugs in Biological Fluids Using SPMEp. 510
SPME-Microcolumn LC: Application to Toxicological Drug Analysisp. 527
Optimization of Drug Analysis by SPMEp. 540
Applications of SPME for the Biomonitoring of Human Exposure to Toxic Substancesp. 557
Applications of SPME in Criminal Investigationsp. 573
Reaction Monitoring
SPME-GC-MS Detection Analysis of Maillard Reaction Productsp. 585
SPME Investigation of Intermediates Produced during Biodegradation of Contaminated Materialsp. 609
Related Techniques
Infrared Spectroscopic Detection for SPMEp. 625
SPME in Near-IR Fiber-optic Evanescent Field Absorption Spectroscopy: A Method for Rapid, Remote In situ Monitoring of Nonpolar Organic Compounds in Waterp. 638
Subject Indexp. 654
Table of Contents provided by Blackwell. All Rights Reserved.

ISBN: 9780854045259
ISBN-10: 0854045252
Series: RSC Chromatography Monographs
Audience: Professional
Format: Hardcover
Language: English
Number Of Pages: 674
Published: 23rd April 1999
Country of Publication: GB
Dimensions (cm): 24.77 x 17.15  x 4.45
Weight (kg): 1.09

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